ARL QUANT’X EDXRF

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Thermo Scientific ARL QUANT’X
The peak of EDXRF performance

The Thermo Scientifi c ARL QUANT’X Energy-Dispersive X-ray Fluorescence spectrometer is a state-of-the-art elemental analyzer for the most challenging analytical tasks in research and manufacturing.

Technical Specifications

X-ray GeneratorAvailable X-ray Detectors
Tube Target:Rh standard, Ag optionalDetector Type:Silicon drift detector (SDD)
X-ray Power:50 W maximumCooling:Thermoelectric cooling (Peltier)
Voltage Range:4-50 kV in 1 kV stepsActive Area:30 mm2
Current Range:0.02-1.98 mA in 0.02 mA stepsActive Depth:1 mm (1000 microns)
Cooling:Air-cooledEnergy Resolution:< 155 eV at 5.9 keV
Selectivity:8 filter positionsWindow Material:Beryllium
Beam Size:1.0 mm – 8.8 mm, user adjustableWindow Thickness:12.5 micron
Basic PerformanceSensitivity:Fluorine to uranium
Stability:< 0.3% rsd over 8 hoursDetector Type:Si(Li) detector
Sensitivity:< 3 ppm for Fe and Pb in Conostan S12Cooling Type:Thermoelectric cooling (Peltier)
Stray Lines:< 0.015% med eV, < 0.05% high eVCrystal Area:15 mm2
Repeatability:< 0.3% rsd at 1 million countsCrystal Depth:3.5 mm (3500 microns)
Sample ChamberEnergy Resolution:< 155 eV at 5.9 keV
Sample Size:30.0 cm x 40.0 cm x 5.0 cm maximumWindow Material:Beryllium
Extension 1:20.0 cm max. sample heightWindow Thickness:8 micron
Extension 2:36.0 cm max. sample heightSensitivity:Fluorine to Uranium
Atmosphere:Air, Vacuum and Helium optionPulse Processor
Sample holder:1-sample stage and large deckProcessor Type:32-bit Digital, 3 DSP
Auto-samplers:10- and 20-position sample traysChannels:2048, 20 eV / channel
Special Stages:R-Theta (disk) and Y-Theta (wafer)Shaping Time:2-20 μs, user adjustable
Sample Imaging:CCD Camera, VGA resolutionCount Rate:Up to 100,000 cps (ICR)
Sample-spinner:Available, software-controlledEnergy Range:400 eV - 40960 eV
Helium Flush:15-65 psig input, 2.4 liters/min max.Deadtime effect:< 3.0%
Radiation and Electrical Safety
Pileup correction:< 0.3%
Interlocks:Chamber lid (dual, separate circuits),
X-ray tube, detector, warning light,
side panels. Fail-safe circuit design.		Calibration:Software-controlled
Radiation:< 0.25 mR/hr at a distance of 2 inchesSite / Utility Requirements
Sound:< 65 dbA at a distance of 1 meterLine Voltage:110-240 VAC, 50/60 Hz
Compliance:TÜV, UL, CE, GSSpectrometer:500 W
Computer and SoftwareVacuum Pump:1000 W
PC Platform:Laptop or Desktop computerAmbient Temp:0-30°C (32-86°F)
Processor:Intel Core FamilyHumidity:20-80%, non-condensing
Memory:4 GB RAM, 250 GB hard driveConditions:Indoor use only
Communication:Ethernet (2 ports), USBWeight and Dimensions
Operating System:Windows® 7Height:42.7 cm (closed), 91.5 cm (open)
Elemental Range:F-U, no limit on number of analytesWidth x Depth:72.4 cm x 59.7 cm
Exc. Conditions:Up to 8 conditions per sampleWeight:80-91 kg (175-200 lbs), approx.
Spectrum Display:Auto-peak ID, KLM markers, conditions
and status, overlays, hardware control
Peak Processing:Peak-profile XML fit, background filter
Standard Analysis:Linear, quadratic, ratio, intensity or conc.
correction, comprehensive custom FP.
Advanced Quant:UniQuant FP for multi-matrix
standardless analysis, full sample
property correction, drift correction,
factory precalibrated

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ARL QUANT'X EDXRF​
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ARL PERFORMX WDXRF

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A New Evolutionary Platform

The Thermo Scientific ARL PERFORM’X X-ray fluorescence (XRF) sequential spectrometer presents an advanced platform for rapid and precise analysis of up to 90 elements in nearly any solid or liquid sample. Advantages over other analytical techniques are:
  • Easy and fast sample preparation
  • Analysis of the whole surface of a sample, a segment of it or specific spots on the surface
  • Speed of analysis
  • High stability and excellent precision
  • Wide dynamic range (from ppm levels to 100%)
  • Simple and rapid analysis of totally unknown samples through advanced standard-less analysis packages
    • The ARL PERFORM’X spectrometer new compact design provides superior benefits of XRF analysis including sensitivity, reproducibility and ease of use while establishing new standards of speed, reliability and flexibility on the widest range of sample types. It will solve composition problems in demanding industrial processes and quality applications in industries as diverse as metallurgy, petroleum, polymers, mining, glass, cement and refractories. Academic or research labs dealing with geochemistry, automotive engineering, materials science, environmental research and forensics will benefit from its performance and versatility.

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    ARL PERFORMX WDXRF
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    ARL OPTIMX-Series-WDXRF-Spectrometer-OPTIMXCEMENT

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    amazing performance in WDXRF

  • 200 W analytical performance from 50 W power
  • 500 W analytical performance from 200 W power
    • Wavelength dispersive X-ray fluorescence (WDXRF) is one of the most versatile analytical methods for elemental analysis of solids and liquids. Elements from boron to uranium can be analyzed in a wide variety of samples with high accuracy, precision and reliability. The technique and the analytical methods are mature enough to establish clear qualitative and quantitative characterization of diversified materials. Modern technological developments have helped to include WDXRF into standard test methods for analytical laboratories (ASTM and ISO norms for example) by virtue of its simplicity, flexibility, affordability and reliability. The cost per analysis is clearly advantageous over many traditional wet chemical and other spectroscopic methods.

    Specifications of the Thermo Scientific ARL OPTIM’X XRF spectrometer

    Element rangeFluorine (Z=9) to uranium (Z=92) with 2 detectors fitted. Fluorine to Iron (Z=26) with FPC detector fitted
    (Carbon (Z=6) can be fitted as fixed channel)
    Spectrometer environmentVacuum for solids, helium for liquids and loose powders
    Spectrometer designAnalysis devices contained in a temperature controlled vacuum chamber made of grey cast iron
    Spectrometer arrangementX-ray tube inclined at 66° under sample for optimum incidence
    Spectrometer capacitySimultaneous configuration: Four Multichromators (covering eight elements)
    Sim-seq configuration: SmartGonio + one Multichromator (covering two elements)
    UCCO technologyUltra Closely Coupled Optics offering largest solid angle for most efficient irradiation of the total sample surface: 50 W power providing
    excitation similar to 200 W or 200 W power providing excitation similar to 500 W
    X-ray excitationAir cooled Rh anode end window tube with thin Be window (0.075 mm). Other anodes available on request. 50 W version: Solid-state
    high frequency generator of maximum voltage 50 kV and maximum current 2 mA (combinations to be chosen to be at 50 W)
    200 W version: maximum voltage 50 kV and maximum current 10 mA (combinations to be chosen to be at 200 W). Max. line
    voltage variation 230 V -15% to +10%. Stability ± 0.0002% per 1% variation
    SmartGonioFully automatic, gearless, microprocessor controlled compact goniometer using optical encoders
    Total angle range: 0 ˚ -150 ˚ 2 θ (Flow proportional counter: 17 ˚ -150 ˚, Scintillation counter: 0 ˚- 90 ˚ ).
    Continuous digital scans: from 0.25 ˚/min to 327 ˚/min.
    MultichromatorFixed channel using dual curved crystal optics allowing analysis of two elements simultaneously. Sealed detectors available for all
    elements from sodium (Z=11). Flow proportional or scintillation detectors also available depending on element. Dual pulse height
    integration to discriminate and correct for 2nd order peaks. Note: some elements can only be fitted as single channel monochromator
    Counting electronicsMulti-channel analyzer to discriminate peaks of higher energies. Digital Automatic Gain Control (AGC) for pulse shrinking correction.
    Automatic dead time correction ensures linearity of response up to 2 Mcps on flow proportional counter and 1.5 Mcps on scintillation counter
    Sample loadingBasic: 1 position for cassette or liquid cell. Optional: 13 position autosampler
    AutomationARL SMS-Omega full automation with transport link from/to fully automatic sample preparation machines for pressed pellets or fused
    beads or solids
    Sample holdersSample cassettes with maximum size of sample: height 26 mm, diameter 52 mm. Liquid cell: height 22 mm, external diameter 40 mm
    Exposed opening: 29 mm diameter (basic). Rotation of sample holder in analysis position: 6 to 60 rpm
    Dimensions and weightH 126 cm, W 88 cm, D 82 cm with basic sample loading. System weight: approximately 260 kg
    Laboratory informationOptional phone service support through modem connection
    Power requirements1.5 kVA single phase at 50 W; 1.7 kVA single phase at 200 W
    Safety standards
    Electrical and protectionEN IEC 61010-1 (Safety requirements for electrical equipment for measurement, control and
    laboratory use. Part 1: General requirements)
    RadiationFull protection system: Swiss directive ORaP RS 814.501 and German directive RöV BGB1.IS.114
    Electro-magnetic immunityEN CEI 61326-1 (Electrical equipment for measurement, control and laboratory use –
    EMC requirements – Part 1: General requirements)
    European directives2006/95/EC (LVD) Low Voltage Directive
    2002/95/EC (RoHS) Restriction of Hazardous Substances Directive
    2002/96/EC (WEEE) Waste Electrical and Electronic Equipment Directive

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    ARL OPTIMX-Series-WDXRF-Spectrometer-OPTIMXCEMENT
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    ARL-Equinox-1000

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    Thermo Scientific ARL EQUINOX 1000

    The Thermo Scientific™ ARL™ EQUINOX 1000 offers very fast measurements compared to other diffractometers due to our unique EQUINOX curved detector that can measure all diffraction peaks simultaneously across a wide angular range. It will take you just a few minutes on most samples to get a complete analysis regardless of your resolution requirements.

    Specifications

    X-ray sourceGenerator: 3500 W (60kV / 60mA - Option 30kV limitation)
    Cu, Co - Standard sealed X-ray tube
    DetectorCurved Position Sensitive X-ray Detector, CPS 180
    Curvature radius: 180mm
    Acquisition in real time over 110° 2Theta
    Goniometric tableNo moving parts: acquisition in asymmetric mode
    Sample holdersFixed, with or without sample rotation
    Reflection or transmission mode
    Zero background sample cup
    Sample changer: 6 or 30 positions
    Thin layer attachment
    OpticMonochromatic (Germanium, Graphite)
    ComputerWindows© 8, 7 Vista, XP
    SoftwareReal time diffractogram display
    Multiple and automatic recording
    Peak search
    Deconvolution with several shapes
    Phase indentification and quantification
    Degree of crystallinity determination
    Cell parameters, crystallite size, lattice strain
    Crystal structure analysis
    Rietveld analysis
    Free open database for search match
    Option: ICDD PDF2 or PDF4 databases
    Power30-32A / 208-230V / 50-60Hz
    Weight~90 kg
    Cooling waterFlow: ~3,5l/min T°C : ~18 / 25°C
    Dimensions996 mm H x 715 mm D x 750 mm W

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    ARL-Equinox-1000
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    ARL-EQUINOX-100

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    Thermo Scientific ARL EQUINOX 100

    The Thermo Scientific™ ARL™ EQUINOX 100 transportable benchtop X-Ray diffractometer provides very fast measurements compared to other diffractometers due to our unique EQUINOX curved detector that can measure all diffraction peaks simultaneously across a wide angular range. It will take you just a few minutes on most samples to get a complete analysis regardless of your resolution requirements.

    Specifications

    X-ray sourceGenerator: 50 W (50kV / 1mA - Option 30kV limitation)
    Micro-focus X-ray tube (Cu, Co, Ag, Mo)
    DetectorCurved Position Sensitive X-ray Detector, CPS 180
    Curvature radius: 180mm
    Acquisition in real time over 110° 2Theta
    Goniometric tableNo moving parts: acquisition in asymmetric mode
    Sample holdersFixed, with or without sample rotation
    Reflection or transmission mode
    Zero background sample cup
    Controlled Atmosphere Reflection Sample Holder
    Gandolfi chamber
    Sample changer: 6 positions
    Thin layer attachment
    OpticMonochromatic (X-ray mirror)
    ComputerWindows© 8, 7 Vista, XP
    SoftwareReal time diffractogram display
    Multiple and automatic recording
    Peak search
    Deconvolution with several shapes
    Phase identification and quantification
    Degree of crystallinity determination
    Cell parameters, crystallite size, lattice strain
    Crystal structure analysis
    Rietveld analysis
    Free open database for search match
    Option: ICDD PDF2 or PDF4 databases
    PowerStandard: 16A/ 110-230V – 50-60Hz
    No external water cooling
    Weight~80 kg
    Dimensions545 mm H x 585 mm D x 680 mm W

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    ARL-EQUINOX-100
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    ARL_9900 WorkStation

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    ARL 9900 IntelliPower Series X-ray Spectrometers

    A complete laboratory in one instrument

    The Thermo Scientific™ ARL™ 9900 IntelliPower™ series of X-ray spectrometers is the most capable and most versatile ever offered for process control. The key to its versatility is the patented technology which allows two X-ray techniques – X-ray fluorescence (XRF) and X-ray diffraction (XRD) to be combined in one instrument. This makes the ARL 9900 highly productive as it can take the place of two separate instruments. It permits the rapid and accurate analysis of solid samples of various kinds. Up to 83 elements (from B to U, 5 to 92 in the Mendeleev table) in concentrations ranging from parts per million to 100% can be detected. Advanced integrated software bestows fast commissioning of new methods and permits quick reporting and storing of the analytical results where it matters most.

    General specifications for ARL 9900 Intellipower

    Element range
    Boron (Nr. 5) to transuranics (>Nr. 92) providing all necessary crystals are fitted on a universal goniometer. Fluorine (Nr. 9) to transuranics (>Nr. 92) with SmartGonio
    Spectrometer environment
    Stabilized vacuum using molecular pump
    Spectrometer design
    Analysis devices contained in a vacuum chamber made of grey cast iron and temperature controlled. Temperature control by a differential heating and cooling system. Crystals regulated to ± 0.1°C.
    Spectrometer arrangement
    X-ray tube mounted vertically at 90° above sample surface. Analytical devices positioned on a 360° ring looking down at the sample surface.
    X-ray tube
    High performance Rh anode end window tube with thin Be window (0.075 mm). Extra thin (0.05 mm) window option further increases sensitivity for light elements. Optional W or Mo anodes.
    Monochromators
    Fixed mechanical systems using curved crystal optics (flat optics for light elements) and flow proportional, sealed or scintillation detectors. Each monochromator has its individual temperature control to ± 0.1°C. For ultra-high countrates, absorbing filters can be fitted. Dual Pulse height integration to discriminate and correct for 2nd order peaks.
    Universal goniometer
    Gearless, microprocessor controlled goniometer using optical encoders. Fully automatic programming of:
  • Up to 9 flat crystals

  • Up to 4 primary collimators: fine, medium, coarse, extra-coarse

  • 2 detectors: scintillation and flow proportional (Ar/CH4 10 %: flow 5 to 10 ml/min)

    • Independent rotation of crystals and detectors Maximum slewing speed: 4800° 2θ/min
    Accuracy of peak positions vs. ASTM table on LiF crystals: 0.015°
    Angular reproducibility < ± 0.0002°
    Angular resolution 0.001°
    Total angle range: 0°-153° 2θ (Flow proportional counter: 17°-153°. Scintillation counter: 0°-115°)
    Continuous digital scans: from 0.25°/min to 327°/min as function of measuring time and increment.
    Step scan range: Minimum step: 0.001°.
    Maximum practical: 1.00°
    Time of measurement for each step: 0.1 s. - 655 s.
    SmartGonio
    Gearless, microprocessor controlled compact goniometer using optical encoders. Fully automatic programming of:
  • 3 flat crystals

  • 2 detectors: scintillation and flow proportional (Ar/CH4 10 %: flow 5 to 10 ml/min)

    • Fixed collimator selected according to customer’s application
    Independent rotation of crystals and detectors
    Maximum slewing speed: 5500° 2θ/min
    Accuracy of peak positions vs. ASTM table on LiF crystals: 0.015°
    Angular reproducibility < ± 0.0002°
    Angular resolution 0.001°
    Total angle range: 0°-150° 2θ (Flow proportional counter: 17°-150°. Scintillation counter: 0°-90°)
    Continuous digital scans: from 0.25°/min to 327°/min as function of measuring time and increment.
    Step scan range: Minimum step: 0.001°.
    Maximum practical: 1.00°
    Time of measurement for each step: 0.1 s. - 655 s.
    Free Lime Channel
    Microprocessor-controlled compact X-ray diffraction system for determination of free lime in clinker and slags, limestone additions in cement, hot meal calcination monitoring and quartz in raw meal.
    Compact XRD system
    Microprocessor-controlled compact X-ray diffraction system for determination of phase content in various process monitoring.
    X-ray WorkStation including NeXRD
    Full X-ray diffraction system integrated using Co anode X-ray tube and theta/theta geometry for Rietveld analysis.
  • Includes additional solid state 2 kW high frequency generator. Maximum line voltage variation -15 % to +10 %.
    Stability ± 0.0001 % per 1 % variation. Dimensions: H 59 cm, L 78 cm, W 29 cm

  • Typical capacity of the X-ray WorkStation (no PBF):
    – NeXRD + 12 fixed channels
    – NeXRD + 1 SmartGonio + 6 fixed channels.
    – NeXRD + 1 universal goniometer + 5 fixed channels

  • Cassettes opening of 33mm diameter.

  • Additional weight: 55kg
    • Counting electronics
    Multi-channel analyzer to discriminate peaks of higher energy. Digital Automatic Gain Control (AGC) for pulse shrinkage correction. Automatic dead time correction ensures linearity of response up to 2 Mcps on flow proportional counter, 1.5 Mcps on scintillation counter, 1 Mcps on sealed detectors.
    Sample changer and cassettes
    Basic magazine: 12 cassettes for samples of max. height 40 mm and diameter 60 mm. Large capacity X-Y changer: 98 cassettes for samples of max. height 30 mm and diameter 52 mm or 98 samples on supports for direct introduction. Exposed opening 29 mm diameter (basic). Rotation of cassettes in analysis position: 60 rpm. Large changer is easily retrofittable.
    Primary beam filter
    Up to 4 position programmable primary beam filter for modifying X-ray excitation.
  • Cu: For analysis of Ru, Rh, Pd, Ag and Cd (elements that are interfered by Rh lines from the X-ray tube) in light and variable matrices

  • Al: To improve peak to background ratio on Pb or As in light matrices

  • Others filters on request
    • Laboratory information
    Optional phone service support through Modem connection. Safety standards: Electrical and protection: IEC 1010-1,
    IEC 950. Radiation (fully protected system): ORap (CH) 414.501 and BGB1.I norms (< 1 μSv/h). Electro-magnetic immunity: CENELEC EN 50081-2 + EN 50082-2 (industrial).

    Particular specifications for ARL 9900 IntelliPower 600/1200/2500

    Spectrometer capacity
  • 12 fixed channels or

  • 1 goniometer + 8 fixed channels or

  • 1 goniometer + 1 compact XRD system + 8 fixed channels.
    • X-ray generator for 600 W
    Solid state 600 W high frequency generator of maximum voltage 50 kV and maximum current 20 mA. All kV/mA combinations must be chosen to be less than 600 W. Maximum line voltage variation -15 % to + 10 %. Stability ± 0.0001 % per 1 % variation.
    X-ray generator for 1200 W
    Solid state 1.2 kW high frequency generator of maximum voltage 50 kV and maximum current 40 mA. All kV/mA combinations must be chosen to be less than 1200 W. Maximum line voltage variation -15 % to +10 %. Stability ± 0.0001 % per 1 % variation.
    X-ray generator for 2500 W
    Solid state 2.5 kW high frequency generator of maximum voltage 60 kV and maximum current 100 mA. All kV/mA combinations must be chosen to be less than 2500 W. Maximum line voltage variation -15 % to
    +10 %. Stability ± 0.0001 % per 1 % variation.
    Power requirements
    2.9 kVA single phase for 600 W
    3.5 kVA single phase for 1200 W
    5 kVA single phase for 2500 W
    Cooling system
    Closed circuit for deionised water flowing through liquid/air heat exchanger. Flow is regulated between 0.5 and 5 lt/min according to generator setting (to keep
    X-ray tube temperature constant)
    Dimensions and weight for 600 W and 1200 W
    H 166 cm, D 136.5 cm, W 93 cm with basic sample changer + H 31 cm, L 42 cm,
    W 20 cm. Weight: 760 kg.
    Dimensions and weight for 2500 W
    H 166 cm, D 136.5 cm, W 93 cm with basic sample changer + H 47 cm, L 83.5 cm,
    W 41 cm. Weight: 785 kg.

    Particular specifications for ARL 9900 IntelliPower 3600/4200

    Spectrometer capacity
  • 32 fixed channels or

  • 1 goniometer + 24 fixed channels or

  • 1 goniometer + 1 compact XRD system + 14 fixed channels

    • Up to three goniometers configurations also available.
    X-ray generator for 3600 W
    Solid state 3.6 kW high frequency generator (max. settings: 60 kV-60 mA or 30 kV-
    120 mA). 70 kV option (max. settings:
    70 kV-51 mA or 30 kV-120 mA). All combinations must be chosen to be less than 3600 W. Maximum line voltage variation -15 % to +10 %. Stability ± 0.0001 % per 1 % variation.
    X-ray generator for 4200 W
    Solid state 4.2 kW high frequency generator (max. settings: 60 kV-70 mA or 35 kV-120 mA). Optional top performance generator (max. settings: 70 kV-60 mA or 30 kV-140 mA). All combinations must be chosen to be less than 4200 W. Maximum line voltage variation -15 % to +10 %. Stability
    ± 0.0001 % per 1 % variation.
    Power requirements
    6 kVA single phase for 3600 W
    7 kVA single phase for 4200 W
    Cooling system
    Built-in closed circuit for deionised water flowing through liquid/liquid heat exchanger. External water needed is <18°C, pressure
    ≥ 2 bar, flow is regulated between 0.5 and
    4.5 lt/min according to generator setting (water consumption minimization).
    Dimensions
    H 166 cm, D 136.5 cm, W 93 cm with basic sample changer
    System weight
    750 kg

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    ARL_9900 WorkStation
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